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ReproSil-Pur® (Maisch) |
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Porous spherical silica: 3, 5, 10 µm
Pore diameter: 60, 120, 200, 300 A°
Surface area: 500, 300, 200, 100m2/g
Ultrareines Kieselgel mit modernsten Modifizierungen.
Reinheit>99,999%. Für alle Arten von Proben geeignet.
Ultra pure silica. Purity >99,999%
Suitable for all kind of samples
Great pH-Stability
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ReproSil-Pur ODS-3, 5 µm (150 x 4.6 mm)
Eluent:
100 % Acetonitrile
Flow rate: 1 ml/min. Detection: 280 nm
Sample: Company Dr. Ehrenstorfer, Augsburg, Germany |
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ReproSil-Pur ODS-3, 5 µm (250 x 4.6 mm)
Eluent:
A: 20 mM KH2PO4 pH-6.6
B: 20 mM KH2PO4 pH-6,6 / ACN (80/20)
Gradient: 0-5 min.: 0 % B, 5 - 25 min.: 0 - 75 % B
25-30 min. 75 - 100% B; 30-35 min.: 100%B;
Flow rate: 1 ml/min., Detection: 254 nm
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ReproSil-Pur ODS-3, 5 µm(250x4.6 mm)
Eluent: H20/CH3CN/HCOOH (81:9:10)
Detection: 546 nm,
Flow rate: 1 ml/min.,
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Sample:
1=Delphinidin-3-galactoside, 2=Delphinidin-3-glucoside,
3=Delphinidin-3-rutinoside, 4=Cyanidin-3-glucoside,
5=Cyanidin-3-galactoside, 6=Cyanidin-3-arabinoside,
7=Petunidin-3-glucoside, 8=Peonidin-3-galactoside,
9=Peonidin-3-glucoside, 10=Malvidin-3-galactoside,
11=Peonidin-3-arabinoside, 12=Malvidin-3-glucoside.
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Glutathione
ReproSil-Pur ODS-3,
5 µm, (250 x 4.6 mm)
Eluent:
10mM Na2PO4 pH=2,7 + 50 µm
Na-Octylsulfate, 2% ACN, Flow rate:1ml/min
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ReproSil-Pur 120 ODS-3,
5 µm, (150 x 2 mm)
Eluent:
A=H2O B=ACN
Gradient: in 10 min linear from
15 % to 34 % B, then isocratic up to 45 min. |
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Creatine/Creatinine
ReproSil-Pur ODS-3
5µm (150 x 4 mm)
Eluent: 1 mM Tert-Butyl-NH4Cl in H20
Flow rate: 0,8 ml/min.
Detection: 235 nm |
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ReproSil-Pur ODS-3,
5µm, (250 x 4 mm)
Gradient: A=H20 pH2 (H3PO4) / MeOH
(70/30), B=MeOH
Flow rate: 0,8 ml/min, Detection: 254 nm
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ReproSil-Pur ODS-3,
5µm, (250 x 3 mm)
Antioxidants
(from Butter)
Eluent:
A=Acetic Acid 5%
B=MeOH/ACN (1:1)
Gradient: from 40 % B to 90 % B in 10 min.,
then isocratic for 12 min.
Flow rate: 0,5 ml/min.,
Detection: 280 nm,
Injection: 10 µl,
Temperature: RT |
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ReproSil-Pur ODS-3,
5µm, (250 x 4.6 mm)
Eluent:
A: 2.5 l water + 25 ml TEAP (Fluka) pH=3.2
B: ACN / A (70/30, V/v)
Flow rate: 1 ml/min.
Temperature: 40 C°
Lin Gradient: 20 % - 100 % B in 30 min |
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ReproSil-Pur ODS-3,
5µm, (250 x 4.6 mm)
Flow rate: 1ml/min. Temperature: 45 C°
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1=Desmethylvenlafaxine
2=Desmethylmirtazeptine
3=Milnacipram
4=Venlafaxine
5=Mirtazapine
6=IS
7=Desmethylcitalopram
8=Citalopram
9=Paroxetine
10=Fluvoxamine
11=Norfluoxetine
12=Fluoxetine
13=Sertraline |
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ReproSil-Pur ODS-3,
5µm, (125x4mm)
Flow rate: 0,5 ml/min.
Eluent:
A: 20 mM
K-hydrogensulfate
ACN(82/18)
B: 20 mM
K-Dihydrogensulfate
ACN (60/40)
Gradient: 0-100% in 30 mins., then at 100% |
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Sample:
1=Scoplamine
2=Atropine Sulfate
3=Quinine
4=Sparteine Sulfate
5=Cinchonine
6=Papaverine
7=Narcotine
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